Methyl propionate → Undecenyl alcohol
반응식
C[O:2][C:3](=O)[CH:4]=[CH:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13].COC(=O)CC.[H][H]>CO>[CH:3]([OH:2])=[CH:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13]참가 물질
5
실험 절차
In about the same way as described under Example 2, an experiment was carried out with difference being that 10 ml methyl-undecenoate was included in the autoclave instead of 10 ml methylpropionate, while after 5 min hydrogen was added until a pressure increase of 30 bar was reached. The autoclave was kept at 80° C. for 5 hours giving a yield of 2.4 g methanol and about 1 g 1-undecenol.
후처리
- temperatureincrease of 30 bar
출처 및 근거
- ORD 기록
- ord-c7a6d286cf5845f1924c8c7357de989a
- 출처 데이터셋
- uspto-grants-1990_07
- 특허 번호
- US04939307
반응 노트
불러오는 중…