4-Nitrobenzaldehyde → 3,6-Di(p-nitrostyryl)pyridazine
반응식
[CH3:1][C:2]1[N:3]=[N:4][C:5]([CH3:8])=[CH:6][CH:7]=1.[N+:9]([C:12]1[CH:19]=[CH:18][C:15]([CH:16]=O)=[CH:14][CH:13]=1)([O-:11])=[O:10]>C(OC(=O)C)(=O)C>[N+:9]([C:12]1[CH:19]=[CH:18][C:15]([CH:16]=[CH:1][C:2]2[N:3]=[N:4][C:5]([CH:8]=[CH:16][C:15]3[CH:18]=[CH:19][C:12]([N+:9]([O-:11])=[O:10])=[CH:13][CH:14]=3)=[CH:6][CH:7]=2)=[CH:14][CH:13]=1)([O-:11])=[O:10]참가 물질
4
실험 절차
First, 24 g of 3,6-dimethylpyridazine and 60 g of p-nitrobenzaldehyde were dissolved in 1 liter of acetic anhydride, then heated under reflux so as to obtain 33 g of 3,6-di(p-nitrostyryl)pyridazine.
후처리
- temperatureheated
- temperatureunder reflux so as
출처 및 근거
- ORD 기록
- ord-170eb1cb39f94645ba5f78a4b33499dd
- 출처 데이터셋
- uspto-grants-1990_07
- 특허 번호
- US04945021
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