Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanol → 4-p-Tolylsulfonyl-4-methyl-3-dimethoxymethyl-pentanoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Methyl 4-p-tolylsulfonyl-4-methyl-3-dimethoxymethylpentanoate | HCID 12850320 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 4-p-Tolylsulfonyl-4-methyl-3-dimethoxymethyl-pentanoic acid | HCID 12850317 | — |
반응 단계
1 g of the product of Step A was added to a mixture of 20 ml of ethanol and 20 ml of aqueous 2 N sodium hydroxide solution and the mixture was refluxed for 17 hours and was cooled and poured into water. The mixture was extracted with methylene chloride and the organic phase was evaporated to dryness to obtain 4-p-tolylsulfonyl-4-methyl-3-dimethoxymethyl-pentanoic acid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04390724 |
| 출처 데이터셋 | uspto-grants-1983_06 |
| ORD ID | ord-1f8589769f9842c4948589fc9c8644e6 |
| 출처 메모 | uspto-grants-1983_06 |