Thionyl Chloride → HCID 57707975, 화합물
반응식
[Cl:1][C:2]1[CH:3]=[CH:4][CH:5]=[C:6]2[C:11]=1[N:10]=[C:9]([O:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[C:8]([CH2:19]O)=[CH:7]2.O=S(Cl)[Cl:23]>C(Cl)(Cl)Cl>[Cl:1][C:2]1[CH:3]=[CH:4][CH:5]=[C:6]2[C:11]=1[N:10]=[C:9]([O:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[C:8]([CH2:19][Cl:23])=[CH:7]2참가 물질
4
실험 절차
Prepared according to Procedure C using (8-chloro-2-phenoxyquinolin-3-yl)-methanol (1.0 eq) and SOCl2 (5 eq) in CHCl3 (0.25 M) at rt. 8-chloro-3-(chloromethyl)-2-phenoxyquinoline was obtained after purification as a yellow oil.
후처리
- customPrepared
- customat rt
출처 및 근거
- ORD 기록
- ord-164dc5c0e2f14ce59c49fe306c44b89c
- 출처 데이터셋
- uspto-grants-2012_06
- 특허 번호
- US08193199B2
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