N-methyl-2-pyrrolidone → NMP Methanol

HRID 2169656

반응식

HRID 2169656 반응식
[CH3:1][N:2]1[C:6](=[O:7])[CH2:5][CH2:4][CH2:3]1.CN1[C:14](=[O:15])N(C)CCC1.C1C2NC=C(O[C@@H]3O[C@H](CO)[C@H](O)[C@H](O)[C@H]3O)C=2C(Cl)=C(Br)C=1>CO>[CH3:1][N:2]1[C:6](=[O:7])[CH2:5][CH2:4][CH2:3]1.[CH3:14][OH:15]

참가 물질

5

반응물 3

HCID 13387N-methyl-2-pyrrolidone2회HCID 65181X-GalHCID 816462(1H)-Pyrimidinone, tetrahydro-1,3-dimethyl-2회

생성물 1

HCID 22395687NMP Methanol

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

Add 7 ml of either NMP or DMPU to 1 gram of X-gal and stir until dissolved. Bring to 10 ml with NMP or DMPU (whichever is already used). Add 90 ml of methanol and mix thoroughly.

후처리

  1. dissolutionuntil dissolved
  2. additionmix thoroughly

출처 및 근거

ORD 기록
ord-6fe9ce74632447eeb9f020f6ccd74bed
출처 데이터셋
uspto-grants-2015_06
특허 번호
US09046495B2

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