Diclofenac → HCID 86595983, 화합물

HRID 2170009노트

반응식

HRID 2170009 반응식
[CH:1]1[CH:2]=[CH:3][C:4]([NH:11][C:12]2[C:13]([Cl:19])=[CH:14][CH:15]=[CH:16][C:17]=2[Cl:18])=[C:5]([CH2:7][C:8]([OH:10])=[O:9])[CH:6]=1.[OH-].[Na+].O.O.O.O.O.O.[Cl-].[Sr+2:29].[Cl-]>O.C(O)C.O>[Sr:29].[CH:1]1[CH:2]=[CH:3][C:4]([NH:11][C:12]2[C:17]([Cl:18])=[CH:16][CH:15]=[CH:14][C:13]=2[Cl:19])=[C:5]([CH2:7][C:8]([OH:10])=[O:9])[CH:6]=1

참가 물질

6

반응물 3

HCID 3033DiclofenacHCID 14798Sodium HydroxideHCID 6101868Strontium chloride hexahydrate

생성물 1

HCID 86595983HCID 86595983, 화합물

시약·촉매·용매 2

HCID 962Water용매HCID 19096565Water ethanol용매

실험 절차

Diclofenac (0.35 g, 1.18 mmol) was dissolved in water/ethanol (30 ml, 50:50 (volume)) containing sodium hydroxide (24 mg, 0.59 mmol). A solution of strontium chloride hexahydrate (0.16 g, 0.59 mmol) in water (3 ml) was added. The mixture was stirred for 20 minutes, and the title compound was isolated by filtration and dried. Yield 0.122 g (15%).

출처 및 근거

ORD 기록
ord-2c00fd3408e94559b1aa77ec05525baa
출처 데이터셋
uspto-grants-2015_06
특허 번호
US09050312B2

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