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Ammonium formate → HCID 117643826, 화합물

HRID 2171281
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HRID 2171281 반응식
C([O-])=O.[NH4+].[C:5]([C:7]1[CH:8]=[C:9]([F:49])[C:10]([NH:21][CH:22]2[CH2:27][CH2:26][N:25](C(OCC3C=CC=CC=3)=O)[CH2:24][CH:23]2[N:38]2[C:46](=[O:47])[C:45]3[C:40](=[CH:41][CH:42]=[CH:43][CH:44]=3)[C:39]2=[O:48])=[N:11][C:12]=1[NH:13][C:14]1[CH:15]=[N:16][CH:17]=[C:18]([CH3:20])[CH:19]=1)#[N:6]>[Pd].C(OCC)(=O)C.CO>[O:48]=[C:39]1[C:40]2[C:45](=[CH:44][CH:43]=[CH:42][CH:41]=2)[C:46](=[O:47])[N:38]1[CH:23]1[CH:22]([NH:21][C:10]2[C:9]([F:49])=[CH:8][C:7]([C:5]#[N:6])=[C:12]([NH:13][C:14]3[CH:15]=[N:16][CH:17]=[C:18]([CH3:20])[CH:19]=3)[N:11]=2)[CH2:27][CH2:26][NH:25][CH2:24]1
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참가 물질

5

반응물 2

HCID 2723923Ammonium formate2회HCID 117643277HCID 117643277, 화합물

생성물 1

HCID 117643826HCID 117643826, 화합물수율 52.1%

시약·촉매·용매 2

HCID 23938Palladium촉매2회HCID 21584119Ethylacetate methanol용매

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온도
70 °C

실험 절차

Ammonium formate (6 mg) and 10% Pd/C (6 mg) were added to an ethyl acetate/MeOH (1 ml/1 ml) solution containing benzyl 4-((5-cyano-3-fluoro-6-((5-methylpyridin-3-yl)amino)pyridin-2-yl)amino)-3-(1,3-dioxoisoindolin-2-yl)piperidin-1-carboxylate (37 mg) obtained in the 1st step in a nitrogen atmosphere, followed by heating and stirring at 70° C. for 1 hour. Next, ammonium formate (30 mg) and 10% Pd/C (30 mg) were added to the solution, followed by heating and stirring at 70° C. for 1 hour. The reaction solution was cooled to room temperature and insoluble matter was removed by filtration through Celite. Filter cake was washed with ethyl acetate. The resulting filtrate was mixed with wash liquid. The obtained organic layers were washed with saturated saline and dried over anhydrous sodium sulfate. The solvent was distilled away under reduced pressure. A white solid of 6-((3-(1,3-dioxoisoindolin-2-yl)piperidin-4-yl)amino)-5-fluoro-2-((5-methylpyridin-3-yl)amino)nicotinonitrile (15 mg) was thus obtained.

후처리

  1. customobtained in the 1st step in a nitrogen atmosphere
  2. temperatureby heating
  3. temperatureby heating
  4. stirringstirring at 70° C. for 1 hour
  5. temperatureThe reaction solution was cooled to room temperature
  6. custominsoluble matter was removed by filtration through Celite
  7. filtrationFilter cake
  8. washwas washed with ethyl acetate
  9. additionThe resulting filtrate was mixed
  10. washwith wash liquid
  11. washThe obtained organic layers were washed with saturated saline
  12. dry with materialdried over anhydrous sodium sulfate
  13. distillationThe solvent was distilled away under reduced pressure

출처 및 근거

ORD 기록
ord-5f92f8e901c44d5080cd7aedef5ac329
출처 데이터셋
uspto-grants-2015_06
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US09051310B2

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