Hydrochloric Acid → 3-Chloro-1-(3-isoxazolyl)-1-propanone

HRID 2179987노트

반응식

HRID 2179987 반응식
[O:1]1[CH:5]=[CH:4][C:3]([C:6](=[O:9])[CH:7]=[CH2:8])=[N:2]1.[ClH:10]>CCOCC>[Cl:10][CH2:8][CH2:7][C:6]([C:3]1[CH:4]=[CH:5][O:1][N:2]=1)=[O:9]

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 224899521-(3-Isoxazolyl)-2-propen-1-one

생성물 1

HCID 224890493-Chloro-1-(3-isoxazolyl)-1-propanone

시약·촉매·용매 1

HCID 3283Diethyl Ether용매

실험 절차

The product of step (b) was treated with 1M HCl in ether (5 ml) and stirred for 4 h at ambient temperature. The solvent was then removed under reduced pressure to leave the product as a dark gum (0.42 g).

후처리

  1. customThe solvent was then removed under reduced pressure

출처 및 근거

ORD 기록
ord-734f46ae7d784cbf84eac67a815bea78
출처 데이터셋
uspto-grants-2005_05
특허 번호
US06887871B2

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