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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 2181928생성일: 2026년 10월 26일

Potassium Carbonate → 3-Chloro-5-[(3-methoxyphenyl)sulfonyl]-6-methyl-5,6-dihydrophenanthridine

https://huagongshe.com/reaction/2181928

반응식

참여 물질

역할이름HCID투입량
반응물Potassium CarbonateHCID 11430—
반응물N-[1-(4'-chloro-2'-fluoro-1,1'-biphenyl-2-yl)ethyl]-3-methoxybenzenesulfonamideHCID 22482365—
용매DimethylformamideHCID 6228—
생성물3-Chloro-5-[(3-methoxyphenyl)sulfonyl]-6-methyl-5,6-dihydrophenanthridineHCID 22482385—

반응 단계

The title compound was prepared from N-[1-(4′-chloro-2′-fluoro-1,1′-biphenyl-2-yl)ethyl]-3-methoxybenzenesulfonamide (686 mg, 1.6 mmol), anhydrous N,N-dimethylformamide (2 mL), and potassium carbonate (442 mg, 3.2 mmol) according to the procedure and in the same manner as described in Example 105, step d resulting in the isolation of 547 mg (84%) of a white solid that was used without further purification;

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US06894061B2
출처 데이터셋uspto-grants-2005_05
ORD IDord-450d5ed9802d4dab8c945f1b05285d77
출처 메모uspto-grants-2005_05