HRID2181928

反应详情

EQUATION

反应方程式

HRID 2181928 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The title compound was prepared from N-[1-(4′-chloro-2′-fluoro-1,1′-biphenyl-2-yl)ethyl]-3-methoxybenzenesulfonamide (686 mg, 1.6 mmol), anhydrous N,N-dimethylformamide (2 mL), and potassium carbonate (442 mg, 3.2 mmol) according to the procedure and in the same manner as described in Example 105, step d resulting in the isolation of 547 mg (84%) of a white solid that was used without further purification;