Hydroxyamine hydrochloride → HCID 22556512, 화합물

HRID 2184687노트

반응식

HRID 2184687 반응식
[CH:1]([C:3]1[S:13][C:6]2[NH:7][C:8]([C:10]([OH:12])=[O:11])=[CH:9][C:5]=2[CH:4]=1)=O.Cl.[NH2:15]O>>[C:1]([C:3]1[S:13][C:6]2[NH:7][C:8]([C:10]([OH:12])=[O:11])=[CH:9][C:5]=2[CH:4]=1)#[N:15]

참가 물질

3

반응물 2

HCID 443297Hydroxyamine hydrochlorideHCID 122572012-formyl-6H-thieno[2,3-b]pyrrole-5-carboxylic acid

생성물 1

HCID 22556512HCID 22556512, 화합물

실험 절차

2-Formyl-6H-thieno[2,3-b]pyrrole-5-carboxylic acid (Soth, S. et al., Bull. Soc. Chim. Fr., 2511-2515 (1975)) was treated with hydroxylamine hydrochloride according to Procedure G (100° C. for 13 h, 125° C. for 7 h; after cooling to room temperature, concentration gave crude product).

출처 및 근거

ORD 기록
ord-b252ea1533b4409996bc4072c1660661
출처 데이터셋
uspto-grants-2002_06
특허 번호
US06399601B1

반응 노트

불러오는 중…