Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
6,7,8,9-tetrahydro-5H-benzo(7)annulene-5-carboxylic acid → N-[(1-ethylpyrazol-4-yl)methyl]-N-(4-isopropylphenyl)-6,7,8,9-tetrahydro-5H-benzocycloheptene-5-carboxamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 6,7,8,9-tetrahydro-5H-benzo(7)annulene-5-carboxylic acid | HCID 14822604 | — |
| 반응물 | N-((1-Ethyl-1H-pyrazol-4-yl)methyl)-4-isopropylaniline | HCID 21957909 | — |
| 생성물 | N-[(1-ethylpyrazol-4-yl)methyl]-N-(4-isopropylphenyl)-6,7,8,9-tetrahydro-5H-benzocycloheptene-5-carboxamide | HCID 17854196 | 57% |
반응 단계
By the reaction and treatment in the same manner as in Example 12 using 6,7,8,9-tetrahydro-5H-benzocycloheptene-5-carboxylic acid (0.29 g) and [(1-ethylpyrazol-4-yl)methyl](4-isopropylphenyl)amine (0.37 g) as starting materials, N-[(1-ethylpyrazol-4-yl)methyl]-N-(4-isopropylphenyl)-6,7,8,9-tetrahydro-5H-benzocycloheptene-5-carboxamide (0.36 g) was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08198454B2 |
| 출처 데이터셋 | uspto-grants-2012_06 |
| ORD ID | ord-40128212572a4fbe8a6381a6bddd6a03 |
| 출처 메모 | uspto-grants-2012_06 |