Bromine → HCID 22597763, 화합물

HRID 2187539노트

반응식

HRID 2187539 반응식
[CH3:1][O:2][C:3]1[CH:11]=[C:10]([CH:12]([CH3:14])[CH3:13])[CH:9]=[CH:8][C:4]=1[C:5]([OH:7])=[O:6].[Br:15]Br>C(Cl)(Cl)Cl>[Br:15][C:9]1[C:10]([CH:12]([CH3:14])[CH3:13])=[CH:11][C:3]([O:2][CH3:1])=[C:4]([CH:8]=1)[C:5]([OH:7])=[O:6]

참가 물질

4

반응물 2

HCID 24408BromineHCID 126137372-Methoxy-4-(propan-2-yl)benzoic acid

생성물 1

HCID 22597763HCID 22597763, 화합물

시약·촉매·용매 1

HCID 6212Chloroform용매2회

실험 절차

To a solution of 2-methoxy-4-iso-propyl benzoic acid (7.0 g, 36.0 mmol) in chloroform (100 ml) was added bromine (1.86 ml) in chloroform (20 ml) dropwise. The reaction was stirred at room temperature overnight. Evaporation in vacuo afforded an oil (9.27 g), m/z (CI); 275, 273 (MH−; 70%).

후처리

  1. customEvaporation in vacuo

출처 및 근거

ORD 기록
ord-681108fa6d654f00aea8e4bd5d3d2f06
출처 데이터셋
uspto-grants-2002_06
특허 번호
US06410555B1

반응 노트

불러오는 중…