Sodium Hydroxide → 4-(3,4-Dimethoxybenzoyl)benzoic acid

HRID 2187957노트

반응식

HRID 2187957 반응식
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:18]=[CH:19][C:20]=1[O:21][CH3:22])[C:6]([C:8]1[CH:17]=[CH:16][C:11]([C:12]([O:14]C)=[O:13])=[CH:10][CH:9]=1)=[O:7].[OH-].[Na+]>C(O)C>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:18]=[CH:19][C:20]=1[O:21][CH3:22])[C:6]([C:8]1[CH:17]=[CH:16][C:11]([C:12]([OH:14])=[O:13])=[CH:10][CH:9]=1)=[O:7]

참가 물질

4

반응물 2

HCID 14798Sodium HydroxideHCID 22645197Methyl 4-(3,4-dimethoxybenzoyl)benzoate

생성물 1

HCID 226452014-(3,4-Dimethoxybenzoyl)benzoic acid

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

1.3 g (4.33 mmol) of methyl 4-(3,4-dimethoxybenzoyl)benzoate was dissolved in 50 ml of ethanol. 7 ml of 1 N sodium hydroxide solution was added to the obtained solution, and they were stirred overnight. The solvent was evaporated, and the residue was washed with ethyl acetate and then filtered to obtain the title compound.

후처리

  1. customThe solvent was evaporated
  2. washthe residue was washed with ethyl acetate
  3. filtrationfiltered

출처 및 근거

ORD 기록
ord-098d053346434bc58ad69083a0b2469d
출처 데이터셋
uspto-grants-2002_06
특허 번호
US06410538B2

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