Diphosgene → HCID 59578065, 화합물

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[CH2:1]([C:3]1[CH:8]=[CH:7][C:6]([N:9]2[CH2:13][CH2:12][C:11]3([CH2:18][CH2:17][NH:16][CH2:15][CH2:14]3)[C:10]2=[O:19])=[CH:5][CH:4]=1)[CH3:2].O=C(Cl)[O:22][C:23](Cl)(Cl)Cl.[CH3:28][NH:29][CH2:30][CH2:31][CH3:32]>>[CH3:28][N:29]([CH2:30][CH2:31][CH3:32])[C:23]([N:16]1[CH2:17][CH2:18][C:11]2([C:10](=[O:19])[N:9]([C:6]3[CH:5]=[CH:4][C:3]([CH2:1][CH3:2])=[CH:8][CH:7]=3)[CH2:13][CH2:12]2)[CH2:14][CH2:15]1)=[O:22]

참가 물질

반응물 3

HCID 10426Diphosgene

HCID 12315N-Methylpropylamine

HCID 58287273HCID 58287273, 화합물

생성물 1

HCID 59578065HCID 59578065, 화합물

실험 절차

This material was prepared in analogy to example 251 step B) from 2-(4-Ethyl-phenyl)-2,8-diaza-spiro[4.5]decan-1-one, diphosgene and methyl-propyl-amine. MS (ESI): 358.4 (MH+).

출처 및 근거

ORD 기록: ord-1b8544c970394c7199a6c1dd16202c93
출처 데이터셋: uspto-grants-2012_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08329904B2

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