Phosphorus oxychloride → HCID 66864934, 화합물

HRID 2194454노트

반응식

[CH2:1]([N:3]1[C:8](=[O:9])[CH:7]=[C:6](OC)[CH:5]=[N:4]1)[CH3:2].P(Cl)(Cl)([Cl:14])=O>>[Cl:14][C:6]1[CH:5]=[N:4][N:3]([CH2:1][CH3:2])[C:8](=[O:9])[CH:7]=1

참가 물질

반응물 2

HCID 24813Phosphorus oxychloride

HCID 668656162-Ethyl-5-methoxy-2,3-dihydropyridazin-3-one

생성물 1

HCID 66864934HCID 66864934, 화합물

실험 절차

The title compound, white crystalline solid, MS: m/e=159.1, 161.1 (M+H+), was prepared in accordance with the general method of example 23c by treatment of 2-ethyl-5-methoxy-2H-pyridazin-3-one with phosphorus oxychloride.

출처 및 근거

ORD 기록: ord-9faac5b88d314239ab7db1ce0523dfff
출처 데이터셋: uspto-grants-2012_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08334287B2

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