참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Dextromethorphan Hydrobromide | HCID 5464025 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Dextromethorphan | HCID 5360696 | — |
반응 단계
The Uncoated Dextromethorphan Resin Complex was prepared by first dissolving 95.42 g of dextromethorphan HBr in 0.8 L of purified water heated to 75-80° C., followed by the addition of 175.82 g AMBERLITE IRP-69 resin (anhydrous) under gentle mixing for 4 hours. At the completion, the suspension was allowed to settle, decanted and rinsed with purified water twice and dried in an oven maintained at 50° C. until moisture is around 5%. The dried resin complex was hand sieved through a 40 mesh screen.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08202537B2 |
|---|
| 출처 데이터셋 | uspto-grants-2012_06 |
|---|
| ORD ID | ord-0d07907a57b6429d827bba54a81baba1 |
|---|
| 출처 메모 | uspto-grants-2012_06 |
|---|