Iodoethane → 2-Butyl-6-(2,5-dimethyl-pyrrol-1-yl)-pyridine
반응식
[CH3:1][C:2]1[N:3]([C:8]2[CH:13]=[CH:12][CH:11]=[C:10]([CH3:14])[N:9]=2)[C:4]([CH3:7])=[CH:5][CH:6]=1.[CH2:15](I)[CH2:16][CH3:17].C(I)C>>[CH2:14]([C:10]1[CH:11]=[CH:12][CH:13]=[C:8]([N:3]2[C:2]([CH3:1])=[CH:6][CH:5]=[C:4]2[CH3:7])[N:9]=1)[CH2:15][CH2:16][CH3:17]참가 물질
4
실험 절차
The product from Example 2a 1.0 g, 5.37 mmol) was reacted with propyl iodide 0.55 mL, 5.64 mmol) in place of ethyl iodide following the procedure from Example 2b to give the title compound (790 mg, 64%).
출처 및 근거
- ORD 기록
- ord-bfa0ec23f2f34a69a919898f169d5ee6
- 출처 데이터셋
- uspto-grants-2012_12
- 특허 번호
- US08338605B2
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