Stannous Chloride → 2-(4-Methoxy-phenylsulfanyl)-5-methyl-phenylamine

HRID 2197771노트

반응식

HRID 2197771 반응식
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([S:9][C:10]2[CH:15]=[CH:14][C:13]([CH3:16])=[CH:12][C:11]=2[N+:17]([O-])=O)=[CH:5][CH:4]=1.Cl[Sn]Cl>>[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]([S:9][C:10]2[CH:15]=[CH:14][C:13]([CH3:16])=[CH:12][C:11]=2[NH2:17])=[CH:7][CH:8]=1

참가 물질

3

반응물 2

HCID 24479Stannous ChlorideHCID 602047921-(4-Methoxy-phenylsulfanyl)-4-methyl-2-nitro-benzene

생성물 1

HCID 433496162-(4-Methoxy-phenylsulfanyl)-5-methyl-phenylamine

실험 절차

The product from Example 50a was reduced with SnCl2 following the procedure from Example 1f giving the title compound.

출처 및 근거

ORD 기록
ord-f94424848a294907bfd558e043cad9e3
출처 데이터셋
uspto-grants-2012_12
특허 번호
US08338605B2

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