Propylamine → 4-(4-chloro-2-nitrophenoxy)-N-propylbenzamide

HRID 2197850노트

반응식

HRID 2197850 반응식
[Cl:1][C:2]1[CH:17]=[CH:16][C:5]([O:6][C:7]2[CH:15]=[CH:14][C:10]([C:11](Cl)=[O:12])=[CH:9][CH:8]=2)=[C:4]([N+:18]([O-:20])=[O:19])[CH:3]=1.[CH2:21]([NH2:24])[CH2:22][CH3:23]>>[Cl:1][C:2]1[CH:17]=[CH:16][C:5]([O:6][C:7]2[CH:15]=[CH:14][C:10]([C:11]([NH:24][CH2:21][CH2:22][CH3:23])=[O:12])=[CH:9][CH:8]=2)=[C:4]([N+:18]([O-:20])=[O:19])[CH:3]=1

참가 물질

3

반응물 2

HCID 7852PropylamineHCID 866154944-(4-Chloro-2-nitrophenoxy)benzoyl chloride

생성물 1

HCID 259341484-(4-chloro-2-nitrophenoxy)-N-propylbenzamide수율 100%

실험 절차

The product from Example 126c (1.0 g, 3.2 mmol) was reacted with propan-1-amine (568 mg, 9.61 mmol) for 12 h following the procedure from Example 126d giving the title compound (1.02 g, 100%).

출처 및 근거

ORD 기록
ord-f13a72dd6b26418cbf560c95304a7cdf
출처 데이터셋
uspto-grants-2012_12
특허 번호
US08338605B2

반응 노트

불러오는 중…