2-(3-Methoxyphenyl)-4-methyl-1,3-oxazole → HCID 59679628, 화합물
반응식
C[O:2][C:3]1[CH:4]=[C:5]([C:9]2[O:10][CH:11]=[C:12]([CH3:14])[N:13]=2)[CH:6]=[CH:7][CH:8]=1>Br>[CH3:14][C:12]1[N:13]=[C:9]([C:5]2[CH:4]=[C:3]([OH:2])[CH:8]=[CH:7][CH:6]=2)[O:10][CH:11]=1참가 물질
3
실험 절차
A solution of 2-(3-methoxyphenyl)-4-methyloxazole (1.1 g, 5.79 mmol) in aqueous hydrogen bromide (10 mL, 48% w/w) was heated to 100° C. for 16 h. The mixture was concentrated to give 3-(4-methyloxazol-2-yl)phenol (0.97 g, crude), which was used without purification. LCMS MH+ 176.
후처리
- concentrationThe mixture was concentrated
출처 및 근거
- ORD 기록
- ord-ba6771fb9bb042fd8a3a07edbacda34e
- 출처 데이터셋
- uspto-grants-2016_06
- 특허 번호
- US09359359B2
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