Hydrochloric Acid → HCID 17978210, 화합물

반응식

[CH3:1][N:2]([CH:4]([CH3:6])C)[CH3:3].[ClH:7].[CH3:8][CH2:9][CH2:10][CH2:11][CH2:12]CC>>[ClH:7].[CH3:1][NH+:2]([CH2:4][C:6]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1)[CH3:3]

참가 물질

반응물 3

HCID 313Hydrochloric Acid

HCID 8900Heptane

HCID 70452N,N-Dimethylisopropylamine

생성물 1

HCID 17978210HCID 17978210, 화합물

실험 절차

6 g of N,N-dimethylisopropylamine and 300 ml of heptane were placed under argon in a 500 ml three-necked flask fitted with internal thermometer and gas inlet stopcock. HCl gas from a gas generation apparatus was passed into this reaction mixture for 1 hour. The N,N-dimethylbenzylammonium hydrochloride formed was separated off via a G4 frit, washed with 100 ml of heptane and dried in an oil pump vacuum. 7.4 g (87%) of the desired product were isolated.