Hydrochloric Acid → HCID 57422604, 화합물

반응식

[CH:1]1([C:6]([CH:8]([NH:13]C(=O)OC(C)(C)C)[CH:9]([CH3:12])[CH2:10][CH3:11])=[O:7])[CH2:5][CH2:4][CH2:3][CH2:2]1.[ClH:21]>>[Cl-:21].[CH:1]1([C:6](=[O:7])[CH:8]([NH3+:13])[CH:9]([CH3:12])[CH2:10][CH3:11])[CH2:5][CH2:4][CH2:3][CH2:2]1

참가 물질

반응물 2

HCID 313Hydrochloric Acid

HCID 21952981HCID 21952981, 화합물

생성물 1

HCID 57422604HCID 57422604, 화합물

실험 절차

4 (0.18 g, 0.63 mmol) was dissolved in 2 ml HCl (7 N in dioxane). After completion of the reaction the solvent was removed and the resulting oil was purified by column chromatography on silical gel using a chloroform/methanol/water gradient. The resulting oil was triturated with ether.

후처리

customAfter completion of the reaction the solvent
customwas removed
customthe resulting oil was purified by column chromatography on silical gel
customThe resulting oil was triturated with ether

출처 및 근거

ORD 기록: ord-a73c945cf85441cbbaeb2ba84ab204bc
출처 데이터셋: uspto-grants-2006_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07109347B2

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