참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Hydrogen Bromide | HCID 260 | — |
| 반응물 | 2-Benzyl-6-methoxypyridine | HCID 21942274 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | HCID 178515992 | HCID 178515992 | 70.9% |
반응 단계
A mixture of 59 g of 2-benzyl-6-methoxypyridine and 200 ml of 47% hydrobromic acid was heated under stirring in an oil bath at 100° C. for 7 hours. After standing to cool, 250 ml of water was added and the resulting crystals were filtered, washed with water and dried under reduced pressure, to give 38.9 g of the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07112593B2 |
|---|
| 출처 데이터셋 | uspto-grants-2006_09 |
|---|
| ORD ID | ord-8432c46a7bbf42feb057a7de3b73cea2 |
|---|
| 출처 메모 | uspto-grants-2006_09 |
|---|
