홈MCP워크벤치Skills
홈워크벤치알림마이페이지
llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
  1. 홈
  2. /반응

ethyl (1R,2S)-2-aminocyclohexane-1-carboxylate hydrochloride → Ethyl(1r,2s)-2-aminocyclohexanecarboxylate

HRID 2218565
노트
인쇄 미리보기

반응식

HRID 2218565 반응식
Cl.[CH2:2]([O:4][C:5]([C@@H:7]1[CH2:12][CH2:11][CH2:10][CH2:9][C@@H:8]1[NH2:13])=[O:6])[CH3:3]>[OH-].[Na+]>[CH2:2]([O:4][C:5]([C@@H:7]1[CH2:12][CH2:11][CH2:10][CH2:9][C@@H:8]1[NH2:13])=[O:6])[CH3:3]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

3

반응물 1

HCID 2724641ethyl (1R,2S)-2-aminocyclohexane-1-carboxylate hydrochloride

생성물 1

HCID 818060Ethyl(1r,2s)-2-aminocyclohexanecarboxylate수율 92.2%

시약·촉매·용매 1

HCID 14798Sodium Hydroxide용매

실험 절차

Ethyl-cis-2-amino-1-cyclohexanecarboxylate hydrochloride (750 mg) was suspended in 1 N NaOH (pH =12). The aqueous layer was extracted with CH2Cl2, washed with brine, dried over Na2SO4 and evaporated to give the crude ethyl-cis-2-amino- 1-cyclohexanecarboxylate (570 mg).

후처리

  1. extractionThe aqueous layer was extracted with CH2Cl2
  2. washwashed with brine
  3. dry with materialdried over Na2SO4
  4. customevaporated

출처 및 근거

ORD 기록
ord-0a8bcbe64fde474dac87d58794b79a2c
출처 데이터셋
uspto-grants-2008_08
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US07411093B2

반응 노트

불러오는 중…

이 페이지에서참가 물질실험 절차후처리출처 및 근거반응 노트