3-Aminopyridine → HCID 69236764, 화합물
반응식
[CH2:1]([O:3][C:4]([C:6]1[C:11](Br)=[CH:10][CH:9]=[C:8]([CH:13]2[CH2:15][CH2:14]2)[N:7]=1)=[O:5])[CH3:2].[NH2:16][C:17]1[CH:18]=[N:19][CH:20]=[CH:21][CH:22]=1>[Pd]>[CH2:1]([O:3][C:4]([C:6]1[C:11]([NH:16][C:17]2[CH:18]=[N:19][CH:20]=[CH:21][CH:22]=2)=[CH:10][CH:9]=[C:8]([CH:13]2[CH2:15][CH2:14]2)[N:7]=1)=[O:5])[CH3:2]참가 물질
4
실험 절차
Palladium catalysed arylation of 3-Bromo-6-cyclopropyl-pyridine-2-carboxylic acid ethyl ester with 3-Aminopyridine according to the general procedure described in example 78 step 3 yielded the title compound as a light yellow solid, MS (ISP): m/e=284.4 (M+H+).
출처 및 근거
- ORD 기록
- ord-3092602dba144d8b95f84aa8cef6f1f4
- 출처 데이터셋
- uspto-grants-2008_08
- 특허 번호
- US07414060B2
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