4-Bromoaniline → N-(4-bromophenyl)-2-nitroaniline
반응식
F[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[N+:8]([O-:10])=[O:9].[Br:11][C:12]1[CH:18]=[CH:17][C:15]([NH2:16])=[CH:14][CH:13]=1.C([O-])(C)(C)C.[K+]>CS(C)=O>[Br:11][C:12]1[CH:18]=[CH:17][C:15]([NH:16][C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=2[N+:8]([O-:10])=[O:9])=[CH:14][CH:13]=1참가 물질
5
실험 절차
The product (6.49 g) is obtained according to the method of stage 1 of Example 4, by using 3.73 mL of 2-fluoro-nitrobenzene and 7.31 g of 4-bromoaniline in the presence of 6.36 g of potassium tert-butanolate in 120 mL of DMSO.
출처 및 근거
- ORD 기록
- ord-ff8b1bc6869c4847892cf242936975a7
- 출처 데이터셋
- uspto-grants-2012_06
- 특허 번호
- US08207373B2
반응 노트
불러오는 중…