Water → 2-Difluoromethoxy-6-fluorobenzamidoxime
반응식
[F:1][CH:2]([F:13])[O:3][C:4]1[CH:11]=[CH:10][CH:9]=[C:8]([F:12])[C:5]=1[C:6]#[N:7].Cl.[NH2:15][OH:16].C(=O)([O-])[O-].[Na+].[Na+].O>C(O)C>[F:13][CH:2]([F:1])[O:3][C:4]1[CH:11]=[CH:10][CH:9]=[C:8]([F:12])[C:5]=1[C:6](=[N:15][OH:16])[NH2:7]참가 물질
6
반응 조건
- 온도
- 75 °C
실험 절차
A mixture of 6.4 g of 2-difluoromethoxy-6-fluorobenzonitrile and 3.1 g of hydroxylamine hydrochloride, 2.6 g of sodium carbonate, 7 ml of water and 35 ml of ethanol was stirred for 20 hours at 75° C.
출처 및 근거
- ORD 기록
- ord-a93129c8c2314509a731f865e1fb142c
- 출처 데이터셋
- uspto-grants-2002_07
- 특허 번호
- US06420605B1
반응 노트
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