Acetone → Pyrogallol

HRID 2231171

반응식

HRID 2231171 반응식
[Al].[CH3:2][C:3]([CH3:5])=[O:4].C(OCCOC)(=[O:8])C.[CH2:14]([C:16](C)=[O:17])[CH3:15]>>[C:3]1([CH:5]=[CH:15][CH:14]=[C:16]([OH:17])[C:2]=1[OH:8])[OH:4]

참가 물질

5

반응 조건

온도
70 °C

실험 절차

Both surfaces of a 0.24 mm thick aluminum plate were sand-grained using a nylon brush and an aqueous dispersion of 400 mesh pumice stone and thoroughly washed with water. This aluminum plate was dipped in a 5% aqueous solution of sodium triphosphate maintained at 70° C. for 3 minutes, washed with water, and dried. A photo-sensitive solution as described in British Pat. No. 1,113,759 was prepared by dissolving 1 part by weight of a naphthoquinone-1,2-diazido-5-sulfonic acid ester of polyhydroxyphenyl obtained by polycondensation of acetone and pyrogallol and 2 parts by weight of a novolak type phenol-formaldehyde resin in a mixed solvent of 20 parts by weight of 2-methoxyethyl acetate and 20 parts by weight of methyl ethyl ketone. This photo-sensitive solution was coated on one surface of the above-prepared plate and then on the other surface to produce a pre-sensitized printing plate which has photo-sensitive layers on both surfaces of the plate. The thus-produced printing plate was cut in three 1,003 mm×800 mm pieces to produce Samples A, B and C.

후처리

  1. washan aqueous dispersion of 400 mesh pumice stone and thoroughly washed with water
  2. washwashed with water
  3. customdried
  4. custom1,113,759 was prepared

출처 및 근거

ORD 기록
ord-ca2206a8b45444a98381909e690b2598
출처 데이터셋
uspto-grants-1988_11
특허 번호
US04781941

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