Triethylamine → N,N,N'-triphenyl-N'-4-pyridinylurea

HRID 2231231

반응식

HRID 2231231 반응식
[C:1]1([NH:7][C:8]2[CH:13]=[CH:12][N:11]=[CH:10][CH:9]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C(N(CC)CC)C.[C:21]1([N:27]([C:31]2[CH:36]=[CH:35][CH:34]=[CH:33][CH:32]=2)[C:28](Cl)=[O:29])[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1>C(Cl)(Cl)Cl>[C:21]1([N:27]([C:31]2[CH:36]=[CH:35][CH:34]=[CH:33][CH:32]=2)[C:28]([N:7]([C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[C:8]2[CH:9]=[CH:10][N:11]=[CH:12][CH:13]=2)=[O:29])[CH:22]=[CH:23][CH:24]=[CH:25][CH:26]=1

참가 물질

5

반응물 3

HCID 8471TriethylamineHCID 65741N,N-Diphenylcarbamic chlorideHCID 89945N-phenylpyridin-4-amine

생성물 1

HCID 14302814N,N,N'-triphenyl-N'-4-pyridinylurea

시약·촉매·용매 1

HCID 6212Chloroform용매2회

실험 절차

A solution of 8.51 g (0.05 mol) of N-phenyl-4-pyridinamine in 400 ml of chloroform is mixed with 11.5 g (0.11 mol) of triethylamine. To this mixture is added, dropwise with stirring, a solution of 11.6 G (0.05 mol) of diphenylcarbamic chloride in chloroform.

후처리

  1. additionTo this mixture is added

출처 및 근거

ORD 기록
ord-e89a5c769b7a4fa2a44cf30d19b26566
출처 데이터셋
uspto-grants-1988_11
특허 번호
US04782071

연결된 노트

불러오는 중…