Hydrochloric Acid → HCID 59296084, 화합물
반응식
Cl[S:2]([C:5]1[CH:14]=[C:13]2[C:8]([C:9]([C:16]([OH:18])=[O:17])=[CH:10][NH:11][C:12]2=[O:15])=[CH:7][CH:6]=1)(=[O:4])=[O:3].[CH2:19]([CH2:21][NH2:22])[OH:20].Cl>O1CCCC1>[OH:20][CH2:19][CH2:21][NH:22][S:2]([C:5]1[CH:14]=[C:13]2[C:8]([C:9]([C:16]([OH:18])=[O:17])=[CH:10][NH:11][C:12]2=[O:15])=[CH:7][CH:6]=1)(=[O:4])=[O:3]참가 물질
5
실험 절차
7-(Chlorosulfonyl)-1-oxo-1,2-dihydroisoquinoline-4-carboxylic acid (1 g) was added to ethanolamine (3 ml) in tetrahydrofuran (3 ml) and the mixture was stirred for 18 h. Hydrochloric acid was added to acidify the mixture, which was filtered to yield 1,2-dihydro-7-[[(2-hydroxyethyl)amino]sulfonyl]-1-oxo-4 isoquinolinecarboxylic acid as a white solid.
후처리
- filtrationwas filtered
출처 및 근거
- ORD 기록
- ord-ed9055cdd71244e1917487faad8996a7
- 출처 데이터셋
- uspto-grants-2010_05
- 특허 번호
- US07709500B2
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