Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Pyridine → HCID 178433931, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Pyridine | HCID 1049 | — |
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | Thioacetamide | HCID 2723949 | — |
| 반응물 | 2,3-Dihydro-3-oxo-6-(4-pyridinyl)-4-pyridazinecarboxylic acid hydrazide | HCID 12790239 | — |
| 용매 | 1-Butanol | HCID 263 | — |
| 생성물 | HCID 178433931 | HCID 178433931 | — |
반응 단계
A mixture of 100 mg of 3-oxo-6-pyridin-4-yl-2,3-dihydro-pyridazine-4-carboxylic acid hydrazide, 130 mg thioacetamide, 87 mg triethylamine, 1 ml of pyridine and 5 ml of butanol is refluxed for 15 hours. After cooling and stirring at room temperature a solid precipitated is collected by filtration, washed with cold isopropanol and dried in vacuo.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07709466B2 |
| 출처 데이터셋 | uspto-grants-2010_05 |
| ORD ID | ord-bbdbd6c97f2c44b9b9dd0ae2b695d54f |
| 출처 메모 | uspto-grants-2010_05 |