N-bromobutanimide → HCID 59299491, 화합물

HRID 2235189노트

반응식

HRID 2235189 반응식
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([Cl:8])=[C:4]([CH3:9])[C:3]=1[Cl:10].[Br:11]N1C(=O)CCC1=O>C(OOC(=O)C1C=CC=CC=1)(=O)C1C=CC=CC=1>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([Cl:8])=[C:4]([CH2:9][Br:11])[C:3]=1[Cl:10]

참가 물질

4

반응물 2

HCID 67184N-bromobutanimideHCID 148011751-Bromo-2,4-dichloro-3-methylbenzene

생성물 1

HCID 59299491HCID 59299491, 화합물수율 99.7%

시약·촉매·용매 1

HCID 7187Benzoyl Peroxide촉매

실험 절차

By the method in Preparation 5 and using the reagents 1-bromo-2,4-dichloro-3-methyl-benzene (74.4 g, 310 mmol), N-bromosuccinimide (58.0 g, 326 mmol) and benzoyl peroxide (750 mg) affords the title compound as an amber oil (98.5 g, 99%):

후처리

  1. customBy the method in Preparation 5

출처 및 근거

ORD 기록
ord-4ff5a07d66f74ddfa7c42412c90483b5
출처 데이터셋
uspto-grants-2010_05
특허 번호
US07713979B2

반응 노트

불러오는 중…