Ethanol → 2-Ethylmercapto-3-ethylbenzoxazolium p-toluenesulfonate
반응식
[SH:1][C:2]1[O:3][C:4]2[CH:10]=[CH:9][CH:8]=[CH:7][C:5]=2[N:6]=1.[C:11]1([CH3:23])[CH:16]=[CH:15][C:14]([S:17]([O:20]CC)(=[O:19])=[O:18])=[CH:13][CH:12]=1.[CH2:24](O)[CH3:25]>>[CH2:11]([S:1][C:2]1[O:3][C:4]2[CH:10]=[CH:9][CH:8]=[CH:7][C:5]=2[N+:6]=1[CH2:24][CH3:25])[CH3:12].[CH3:23][C:11]1[CH:16]=[CH:15][C:14]([S:17]([OH:20])(=[O:19])=[O:18])=[CH:13][CH:12]=1참가 물질
4
반응 조건
- 온도
- 150 °C
실험 절차
A mixture of 3.0 g of 2-mercaptobenzoxazole and 12.0 g of ethyl p-toluenesulfonate was heated to 150° C. to react them for 6 hours. The reaction product was cooled to 80° C., and 25 ml of ethanol was added to it, thereby producing an ethanol solution of 2-ethylmercapto-3-ethylbenzoxazolium-p-toluenesulfonate.