Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → 4-Oxo-2-adamantyl chloromethyl ether
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Formaldehyde | HCID 712 | — |
| 반응물 | 4-Hydroxyadamantan-2-one | HCID 533435 | — |
| 생성물 | 4-Oxo-2-adamantyl chloromethyl ether | HCID 23150860 | — |
반응 단계
Paraformaldehyde was added to 4-oxo-2-hydroxyadamantane, and a hydrogen chloride gas was injected at 2.5 equivalent amounts per this 4-oxo-2-hydroxyadamantane. Then, the reaction was conducted at a temperature of 50° C. for 12 hours. After the completion of the reaction, the product was distillated under reduced pressure so as to obtain 4-oxo-2-adamantyl chloromethyl ether (compound 1) represented by the following chemical formula (58).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07723007B2 |
| 출처 데이터셋 | uspto-grants-2010_05 |
| ORD ID | ord-de9da7268278471faa1a361f851be596 |
| 출처 메모 | uspto-grants-2010_05 |