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Hydrochloric Acid → HCID 10932491, 화합물

HRID 2239204
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HRID 2239204 반응식
[CH2:1]=[O:2].O[CH:4]1[CH:11]2[CH2:12][CH:7]3[CH2:8][CH:9]([CH2:13][CH:5]1[CH2:6]3)[CH2:10]2.[ClH:14]>>[Cl:14][CH2:1][O:2][CH:4]1[CH:11]2[CH2:12][CH:7]3[CH2:8][CH:9]([CH2:13][CH:5]1[CH2:6]3)[CH2:10]2
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참가 물질

4

반응물 3

HCID 313Hydrochloric AcidHCID 712FormaldehydeHCID 641492-Adamantanol2회

생성물 1

HCID 10932491HCID 10932491, 화합물

실험 절차

Paraformaldehyde was added to 2-hydroxyadamantane, and a hydrogen chloride gas was injected at 2.5 equivalent amounts per this 2-hydroxyadamantane. Then, the reaction was conducted at a temperature of 50° C. for 12 hours. After the completion of the reaction, the product was distillated under reduced pressure so as to obtain 2-adamantyl chloromethyl ether (compound 2) represented by the following chemical formula (59).

후처리

  1. customAfter the completion of the reaction

출처 및 근거

ORD 기록
ord-4e5c2b198e7a46519b3199088e4b4b0d
출처 데이터셋
uspto-grants-2010_05
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US07723007B2

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