Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Iodine → HCID 178506332, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Iodine | HCID 807 | — |
| 반응물 | Dicerium ammonium nitrate | HCID 86617141 | — |
| 반응물 | 3-(pentafluoroethyl)-1H-pyrazole | HCID 178506326 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | HCID 178506332 | HCID 178506332 | 162.7% |
반응 단계
An acetonitrile solution (20 ml) of 3-pentafluoroethyl-1H-pyrazole (2.0 g), dicerium ammonium nitrate (3.0 g) and iodine (1.6 g) was refluxed for 3 hours. After cooling, the reaction solution was washed with saturated aqueous solution of sodium thiosulfate and saturated aqueous solution of sodium chloride. After drying the organic layer with magnesium sulfate, the solvent was distilled off under the reduced pressure to obtain 4-iodo-3-pentafluoroethyl-1H-pyrazole (3.2 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07674807B2 |
| 출처 데이터셋 | uspto-grants-2010_03 |
| ORD ID | ord-616beeebfdde422abc9d876986fc83e7 |
| 출처 메모 | uspto-grants-2010_03 |