Hydrazine hydrate (1:1) → 3-(2-Methylphenyl)-6,7,8,9-tetrahydro-5H-cyclohepta[c]pyridazine

HRID 2243930

반응식

HRID 2243930 반응식
[C:1]1(=O)[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][C:2]1=O.COP([CH2:16][C:17](=O)[C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][C:19]=1[CH3:24])(=O)OC.O.[NH2:27][NH2:28]>>[C:19]1([CH3:24])[CH:20]=[CH:21][CH:22]=[CH:23][C:18]=1[C:17]1[N:28]=[N:27][C:2]2[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][C:1]=2[CH:16]=1

참가 물질

4

반응물 3

HCID 24654Hydrazine hydrate (1:1)HCID 763651,2-CycloheptanedioneHCID 14302186Dimethyl 2-o-methylphenyl-2-oxoethylphosphonate

생성물 1

HCID 160637043-(2-Methylphenyl)-6,7,8,9-tetrahydro-5H-cyclohepta[c]pyridazine

실험 절차

light yellow solid. MS (EI): 238.2 (M+). Prepared from cycloheptane-1,2-dione, (2-Oxo-2-o-tolyl-ethyl)-phosphonic acid dimethyl ester, hydrazine monohydrate.

출처 및 근거

ORD 기록
ord-2eedc4efd0d74f959c8890c75d1a6a7e
출처 데이터셋
uspto-grants-2010_03
특허 번호
US07678795B2

연결된 노트

불러오는 중…