Hydrazine hydrate (1:1) → 3-(2,3-Dichlorophenyl)-5,6,7,8-tetrahydro-5,8-methanocinnoline
반응식
[CH:1]12[CH2:7][CH:4]([CH2:5][CH2:6]1)[C:3](=O)[C:2]2=O.COP([CH2:16][C:17]([C:19]1[CH:24]=[CH:23][CH:22]=[C:21]([Cl:25])[C:20]=1[Cl:26])=O)(=O)OC.O.[NH2:28][NH2:29]>>[Cl:26][C:20]1[C:21]([Cl:25])=[CH:22][CH:23]=[CH:24][C:19]=1[C:17]1[N:28]=[N:29][C:2]2[CH:1]3[CH2:7][CH:4]([C:3]=2[CH:16]=1)[CH2:5][CH2:6]3참가 물질
4
실험 절차
yellow viscous oil. MS (ESI): 291.0 (MH+). Prepared from bicyclo[2.2.1]heptane-2,3-dione, [2-(2,3-Dichloro-phenyl)-2-oxo-ethyl]-phosphonic acid dimethyl ester, hydrazine monohydrate.
출처 및 근거
- ORD 기록
- ord-758043ba275742df8f9e6b0899214618
- 출처 데이터셋
- uspto-grants-2010_03
- 특허 번호
- US07678795B2
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