Triethyl Citrate → Ethyl Acetoacetate
반응식
C(OCC)(=O)[CH2:2][C:3]([CH2:10][C:11]([O:13][CH2:14][CH3:15])=[O:12])(C(OCC)=O)[OH:4]>CC([O-])C.CC([O-])C.CC([O-])C.CC([O-])C.[Ti+4]>[C:11]([O:13][CH2:14][CH3:15])(=[O:12])[CH2:10][C:3]([CH3:2])=[O:4]참가 물질
3
실험 절차
In the same way as in Example 1, 60 g (0.21 mol) of tetraisopropyl titanate were reacted with 116.6 g (0.42 mol) of triethyl citrate. The mixture was freed of alcohol under vacuum and 154.6 g of a clear, pale yellow liquid was obtained.
후처리
- customwas obtained
출처 및 근거
- ORD 기록
- ord-0b1f2e1c0f294ff991c72bb3ca95134c
- 출처 데이터셋
- uspto-grants-1995_06
- 특허 번호
- US05428103
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