Azobisisobutyronitrile → Acrylamido methyl-7-hydroxy-4-methyl coumarin stearyl methacrylate

HRID 224685

반응식

HRID 224685 반응식
[Pb].[N].[C:3]([NH:7][CH2:8][C:9]1[C:10](=[O:21])[O:11][C:12]2[C:17]([C:18]=1[CH3:19])=[CH:16][CH:15]=[C:14]([OH:20])[CH:13]=2)(=[O:6])[CH:4]=[CH2:5].[C:22]([O:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][CH3:45])(=[O:26])[C:23]([CH3:25])=[CH2:24].N(C(C)(C)C#N)=NC(C)(C)C#N>CN(C)C=O>[C:3]([NH:7][CH2:8][C:9]1[C:10](=[O:21])[O:11][C:12]2[C:17]([C:18]=1[CH3:19])=[CH:16][CH:15]=[C:14]([OH:20])[CH:13]=2)(=[O:6])[CH:4]=[CH2:5].[C:22]([O:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][CH3:45])(=[O:26])[C:23]([CH3:25])=[CH2:24]

참가 물질

6

반응물 4

HCID 6547AzobisisobutyronitrileHCID 122600Stearyl methacrylateHCID 86733970Acrylamido methyl 7-hydroxy-4-methyl coumarinHCID 178514658HCID 178514658, 화합물

생성물 1

HCID 86733969Acrylamido methyl-7-hydroxy-4-methyl coumarin stearyl methacrylate

시약·촉매·용매 1

HCID 6228Dimethylformamide용매

실험 절차

Into a 50 ml flask provided with a condenser, a nitrogen lead in tube and an agitator, there are introduced 1 g of acrylamido methyl 7-hydroxy-4-methyl coumarin, 2 g of stearyl methacrylate, 0.3 g of azobis-isobutyronitrile and 6 g of dimethylformamide.

후처리

  1. customInto a 50 ml flask provided with a condenser

출처 및 근거

ORD 기록
ord-d72713b400b647d5a7fe368794ba1108
출처 데이터셋
uspto-grants-1980_11
특허 번호
US04233430

연결된 노트

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