Methanol → HCID 14133519, 화합물
반응식
[CH3:1][O:2][C:3](=[O:6])[CH2:4]Br.[O-:7][C:8]#[N:9].[K+].[CH3:11][OH:12]>CN(C=O)C>[CH3:1][O:2][C:3](=[O:6])[CH2:4][NH:9][C:8]([O:12][CH3:11])=[O:7]참가 물질
5
실험 절차
10.71 grams of monobromo acetic acid methyl ester, 8.52 grams of potassium cyanate and 7.85 grams of methanol were heated in 70 ml of DMF following the procedure of Example 1 gave 6.62 grams (64.3%) of methoxycarbonylamino acetic acid methyl ester having a boiling point of 67°-8° C./0.0013 mbar.
출처 및 근거
- ORD 기록
- ord-05549a776bd743fbaa64dcd7bca35360
- 출처 데이터셋
- uspto-grants-1980_11
- 특허 번호
- US04234744
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