Hydrochloric Acid → 4-(Benzhydryl-amino)-butylamine

HRID 2251950노트

반응식

HRID 2251950 반응식
C(OC(=O)[NH:7][CH2:8][CH2:9][CH2:10][CH2:11][NH:12][CH:13]([C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1)[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)(C)(C)C.Cl>CO>[CH:13]([NH:12][CH2:11][CH2:10][CH2:9][CH2:8][NH2:7])([C:20]1[CH:21]=[CH:22][CH:23]=[CH:24][CH:25]=1)[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 53775424N-[4-(benzhydryl-amino)-butyl]-carbamic acid tert-butyl ester

생성물 1

HCID 124911934-(Benzhydryl-amino)-butylamine

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

Batch size: 4.6 g (<11.3 mmol) N-[4-(benzhydryl-amino)-butyl]-carbamic acid tert-butyl ester and 5.2 ml (63 mmol) concentrated hydrochloric acid in 50 methanol.

출처 및 근거

ORD 기록
ord-74bc526abee44844a1bcd63a19f219c9
출처 데이터셋
uspto-grants-2008_01
특허 번호
US07320993B1

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