Thionyl Chloride → HCID 10799500, 화합물

HRID 2254403노트

반응식

HRID 2254403 반응식
[CH2:1]([C:9]1[CH:10]=[C:11]([CH:14]=[CH:15][CH:16]=1)[CH2:12]O)[CH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.S(Cl)([Cl:19])=O>C(Cl)(Cl)Cl>[CH2:1]([C:9]1[CH:10]=[C:11]([CH:14]=[CH:15][CH:16]=1)[CH2:12][Cl:19])[CH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1

참가 물질

4

반응물 2

HCID 24386Thionyl ChlorideHCID 10488743Benzenemethanol, 3-(2-phenylethyl)-

생성물 1

HCID 10799500HCID 10799500, 화합물수율 99%

시약·촉매·용매 1

HCID 6212Chloroform용매

실험 절차

The resulting alcohol (140 mg) was dissolved in 1 ml of chloroform, and 0.3 ml of thionyl chloride was added. The mixture was reacted at room temperature for 30 minutes. The reaction mixture was evaporated under reduced pressure to give 150 mg (yield 99%) of 3-phenethylbenzyl chloride as a pale yellow oil.

후처리

  1. customThe mixture was reacted at room temperature for 30 minutes
  2. customThe reaction mixture was evaporated under reduced pressure

출처 및 근거

ORD 기록
ord-e0d091f11e3940e6979b2fad10b58995
출처 데이터셋
uspto-grants-1993_08
특허 번호
US05234946

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