Sodium Hydroxide → Isotridecanoic acid

반응식

[CH2:1]([OH:14])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH:11]([CH3:13])[CH3:12].[OH-:15].[Na+]>>[C:1]([OH:15])(=[O:14])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH:11]([CH3:12])[CH3:13]

참가 물질

반응물 2

HCID 14798Sodium Hydroxide

HCID 33865Isotridecan-1-ol

생성물 1

HCID 33002Isotridecanoic acid

반응 조건

온도: 340 °C

실험 절차

180 kg of isotridecyl alcohol and 33.6 kg of NaOH were introduced into the 350 liter reactor and heated to 340° C. under a nitrogen pressure of 6 bar. The process was otherwise carried out as described in Example 1. The product obtained had an acid value of 240 and an OH value of 6.3.

후처리

customThe product obtained

출처 및 근거

ORD 기록: ord-f441da02fbca4202b1a3755c32f10e74
출처 데이터셋: uspto-grants-1997_08
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05654453

반응 노트

불러오는 중…