O-Xylene → HCID 18788042, 화합물

HRID 2258381

반응식

HRID 2258381 반응식
[CH2:1]([N:5](CC(C)=C)[C:6]1[CH:11]=CC=C[CH:7]=1)[CH2:2][CH2:3][CH3:4].[C:16]1([CH3:23])[C:17](C)=[CH:18][CH:19]=[CH:20][CH:21]=1>[Cl-].[Zn+2].[Cl-]>[CH2:1]([N:5]1[C:17]2[C:16](=[CH:21][CH:20]=[CH:19][CH:18]=2)[CH2:23][C:6]1([CH3:11])[CH3:7])[CH2:2][CH2:3][CH3:4]

참가 물질

4

반응물 2

HCID 7237O-XyleneHCID 54010992N-butyl-N-(2-methylprop-2-eneyl)aniline

생성물 1

HCID 18788042HCID 18788042, 화합물

시약·촉매·용매 1

HCID 3007855Zincchloride촉매

실험 절차

A mixture of N-butyl-N-(2-methylprop-2-eneyl)aniline (9.6 parts), zinc chloride (6.12 parts) and xylene (20 parts) was heated under reflux with vigorous stirring for 4.75 hours. The cooled mixture was filtered and the organic phase evaporated to leave 1-butyl-2,2-dimethylindoline (5.3 parts).

후처리

  1. temperaturewas heated
  2. temperatureunder reflux
  3. filtrationThe cooled mixture was filtered
  4. customthe organic phase evaporated

출처 및 근거

ORD 기록
ord-7f603290ea884b37aa05920e12f26970
출처 데이터셋
uspto-grants-1997_08
특허 번호
US05660598

연결된 노트

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