Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hexadecylamine → 3-(Hexadecylamino)propane-1,2-diol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hexadecylamine | HCID 8926 | — |
| 반응물 | Glycidol | HCID 11164 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 3-(Hexadecylamino)propane-1,2-diol | HCID 111007 | — |
반응 단계
Hexadecylamine (5.00 g, 0.024 moles) was dissolved in absolute ethanol, and glycidol (3.07 g, 0.041 moles) was added dropwise. The reaction was refluxed under nitrogen for 4 hours then allowed to stir overnight. After 22 hours of refluxing, the reaction was stopped and a white solid formed during the cooling stage. The solid was recovered and recrystallized in hot hexane. (yield=2.02g)
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05476661 |
| 출처 데이터셋 | uspto-grants-1995_12 |
| ORD ID | ord-04890d8fb6154bda9211bfc8e6c4b477 |
| 출처 메모 | uspto-grants-1995_12 |