反应详情

Hexadecylamine (5.00 g, 0.024 moles) was dissolved in absolute ethanol, and glycidol (3.07 g, 0.041 moles) was added dropwise. The reaction was refluxed under nitrogen for 4 hours then allowed to stir overnight. After 22 hours of refluxing, the reaction was stopped and a white solid formed during the cooling stage. The solid was recovered and recrystallized in hot hexane. (yield=2.02g)

1. temperatureThe reaction was refluxed under nitrogen for 4 hours
2. temperatureAfter 22 hours of refluxing
3. customa white solid formed during the cooling stage
4. customThe solid was recovered
5. customrecrystallized in hot hexane