Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Hydroxide → N-(2,3-dihydroxypropyl)-N-hexadecyl-2-hydroxyoctanamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 반응물 | 3-(Hexadecylamino)propane-1,2-diol | HCID 111007 | — |
| 반응물 | Methyl 2-hydroxyoctanoate | HCID 10487462 | — |
| 생성물 | N-(2,3-dihydroxypropyl)-N-hexadecyl-2-hydroxyoctanamide | HCID 10217103 | — |
반응 단계
N-(2,3-dihydroxypropyl)-hexadecylamine (1.0 g, 3.2 mmoles) and potassium hydroxide (0.01 g, 0.18 mmoles) were heated to 85° C. under vacuum and methyl-2-hydroxyoctanoate (0.55 g, 3.2 mmoles) was added dropwise to the reaction. The reaction was heated under vacuum for 6 hours. A waxy off white solid was obtained (crude yield=1,39 g), and the waxy solid further purified by recrystallization in hot hexane. (Yield=0.88g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05476661 |
| 출처 데이터셋 | uspto-grants-1995_12 |
| ORD ID | ord-a7d2978f0e4e4f0da0d2ac2365b13e60 |
| 출처 메모 | uspto-grants-1995_12 |