Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Glycidol → 1,2-Propanediol, 3-(dodecylamino)-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Glycidol | HCID 11164 | — |
| 반응물 | Dodecylamine | HCID 13583 | — |
| 생성물 | 1,2-Propanediol, 3-(dodecylamino)- | HCID 102496 | — |
반응 단계
Dodecylamine (25.02 g, 0.13 mole) was heated to 85° C. Glycidol (10 g, 0.13 mole) was added dropwise. The reaction solution was heated under nitrogen for 3 hours and was stirred overnight at room temperature. A white solid was obtained (crude yield=33.27 g). The solid was recrystalized from hot hexane (crystallized 10.86 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05476671 |
| 출처 데이터셋 | uspto-grants-1995_12 |
| ORD ID | ord-1154cc03e7904ae0a02dac36e85a2e70 |
| 출처 메모 | uspto-grants-1995_12 |